Standard Test Methods for  Chemical Analysis of Hydraulic Cement

ASTM - ASTM International

ASTM C114-24

Organization:

Year: 2024

Abstract: These test methods cover the chemical analyses of hydraulic cements. Specific chemical test methods are grouped as reference test methods and alternative test methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements and are also required for referee analysis in those cases where conformance to chemical specification requirements are questioned. Apparatus and materials for the test method include balance, weights, glassware and laboratory containers, desiccators, filter paper, crucibles, and muffle furnace. Standard reagents for the test method shall be used within the limits of the specification. These reagents shall include purity agents, water, repackaged reagents, concentrated acids and ammonium hydroxide, nonstandardized solutions, and indicator solutions. Sample preparation and general test procedures shall be followed according to the specification. General procedures include sample weighing, taring of crucibles, weighing of ignited residues, volatilization of platinum, chemical analyses, and calculation. Reporting of analyses shall be of the following order: major components, minor components, and separate determinations. Reference test methods and procedures include determination of insoluble residue, silicon dioxide, ammonium hydroxide group, ferric oxide, phosphorus pentoxide, titanium dioxide, zinc oxide, aluminum oxide, calcium oxide, magnesium oxide, sulfur, loss on ignition, sodium and potassium oxides, manganic oxide, chloride, chloroform-soluble organic substances. Alternative test methods and procedures include determination of calcium oxide, calcium dioxide, magnesium oxide, loss on ignition, titanium dioxide, phosphorus pentoxide, manganic oxide, and free calcium oxide. The standardization used for qualification and for analysis of each constituent shall be determined by valid curve-fitting procedures.

URI: https://yse.yabesh.ir/std/handle/yse/342418

Collections :

ASTM - ASTM International

Download PDF : (525.8Kb)
Show Full MetaData Hide Full MetaData
Statistics

Standard Test Methods for Chemical Analysis of Hydraulic Cement

Show full item record

contributor author	ASTM - ASTM International
date accessioned	2025-09-30T18:06:47Z
date available	2025-09-30T18:06:47Z
date copyright	2024
date issued	2024
identifier other	c0114-24.pdf
identifier uri	https://yse.yabesh.ir/std/handle/yse/342418
description abstract	These test methods cover the chemical analyses of hydraulic cements. Specific chemical test methods are grouped as reference test methods and alternative test methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements and are also required for referee analysis in those cases where conformance to chemical specification requirements are questioned. Apparatus and materials for the test method include balance, weights, glassware and laboratory containers, desiccators, filter paper, crucibles, and muffle furnace. Standard reagents for the test method shall be used within the limits of the specification. These reagents shall include purity agents, water, repackaged reagents, concentrated acids and ammonium hydroxide, nonstandardized solutions, and indicator solutions. Sample preparation and general test procedures shall be followed according to the specification. General procedures include sample weighing, taring of crucibles, weighing of ignited residues, volatilization of platinum, chemical analyses, and calculation. Reporting of analyses shall be of the following order: major components, minor components, and separate determinations. Reference test methods and procedures include determination of insoluble residue, silicon dioxide, ammonium hydroxide group, ferric oxide, phosphorus pentoxide, titanium dioxide, zinc oxide, aluminum oxide, calcium oxide, magnesium oxide, sulfur, loss on ignition, sodium and potassium oxides, manganic oxide, chloride, chloroform-soluble organic substances. Alternative test methods and procedures include determination of calcium oxide, calcium dioxide, magnesium oxide, loss on ignition, titanium dioxide, phosphorus pentoxide, manganic oxide, and free calcium oxide. The standardization used for qualification and for analysis of each constituent shall be determined by valid curve-fitting procedures.
language	English
title	Standard Test Methods for Chemical Analysis of Hydraulic Cement	en
title	ASTM C114-24	num
type	standard
status	Active
tree	ASTM - ASTM International:;2024
contenttype	fulltext
scope	1.1 These test methods cover the chemical analyses of hydraulic cements. Any test methods of demonstrated acceptable precision and bias may be used for analysis of hydraulic cements, including analyses for referee and certification purposes, as explained in Section 4. Specific chemical test methods are provided for ease of reference for those desiring to use them. They are grouped as Reference Test Methods and Alternative Test Methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements. The alternative test methods generally provide individual determination of specific analytes and may be used alone or as alternates and determinations within the basic scheme at the option of the analyst and as indicated in the individual method. 1.2 Contents: Section Subject 2 Referenced Documents 4 Description of Referee Analyses 4.1 Referee Analyses 5 Qualification for Different Analyses 5.1 Certified Reference Materials 5.2 Requirements for Qualification Testing 5.3 Alternative Analyses 5.4 Performance Requirements for Rapid Test Methods 6 General 6.1 Interferences and Limitations 6.2 Apparatus and Materials 6.3 Reagents 6.4 Sample Preparation 6.5 General Procedures 6.6 Recommended Order for Reporting Analyses Reference Test Methods 7 Insoluble Residue 8 Silicon Dioxide 8.2 Cements with Insoluble Residue Less Than 1 % 8.3 Cements with Insoluble Residue Greater Than 1 % 9 Ammonium Hydroxide Group 10 Ferric Oxide 11 Phosphorus Pentoxide 12 Titanium Dioxide 13 Zinc Oxide 14 Aluminum Oxide 15 Calcium Oxide 16 Magnesium Oxide 17 Sulfur 17.1 Sulfur Trioxide 17.2 Sulfide 18 Loss On Ignition 18.1 Portland Cement 18.2 Portland Blast-Furnace Slag Cement and Slag Cement 19 Sodium and Potassium Oxides 19.1 Total Alkalis 19.2 Water-Soluble Alkalis 20 Manganic Oxide 21 Chloride 22 Chloroform-Soluble Organic Substances Alternative Test Methods 23 Calcium Oxide 24 Carbon Dioxide 25 Magnesium Oxide 26 Loss on Ignition 26.1 Portland Blast-Furnace Slag Cement and Slag Cement 27 Titanium Dioxide 28 Phosphorus Pentoxide 29 Manganic Oxide 30 Free Calcium Oxide Appendices Appendix X1 Example of Determination of Equivalence Point for the Chloride Determination Appendix X2 CO2 Determinations in Hydraulic Cements 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
identifier DOI	10.1520/C0114-24